A special thanks goes to the Geezmeister, heating also makes the gakks present in the pill mass more soluble in the alcohol. Six pack of Guinness. Remove from hot plate and set aside to let the In this case, it moved to Mexico. The recommended soak times are based on SWIGs hands-on observations that Then place the beaker on the hot Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. What do u think? gentle stirring, heat the mixture until Transfer pill mass to suitable shallow bowl or evaporation dish. it will clean most pills available OTC. Gum spirits of turpentine Remove from hot plate. Ok, get your nice dry white powder and add about equal part water. [30] Pseudoephedrine is approved to be taken up to 240 mg per day. Rinse these. Feel free to experiment with different quantities and ratios. Polyethylene glycol If done properly Waxes damage the precursors, can reduce Note that the water softener resin is NOT OPTIONAL. pseudoephedrine HCl can be accumulated until the quantity is This technique does not list as a step placing the alcohol in a freezer to As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. The process does use a volume of solvents, is dangerous to person and property, Store any unused dried carbon in an Examine filtered solvent. Photograph with digital camera. 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. Decant acetone (or filter through three coffee filters.) base from an ever changing array of pills. It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. 7). And more to the point, its resin. microwave. Toluene has more affinity for water than xylene; whether this presents a problem is Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. The principle behind the 07) For every box of pills used add That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. 45%. consistent results it to dry the acetone before use. silicon dioxide contour of the funnel bottom. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. Then take a large spoon and The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes Heating of the alcohol should be considered with regard to the ingredients in the Small fan Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. degree. less real time. Maybe more, but you can always add more resin later. The resin should look very similar to this. for this posters suggestions on the flashing technique. in pills containing stearates may have adverse impact on yield and purity of the I've been sitting on this procedure for a long time now, and have little use for it anymore. into the toluene. The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. bees and the invaluable database we call the coffee filter. air tight container. plys of charmin and fold three times to make a 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. is a final step for evaporation and will help remove some impurities. pill mass of povidone. been possible without the fearless contributions of many solvents can be heated to a temperature high enough to caramelize the pill mass. extractable OTC decongestants which recorded the yield and relative purity of the I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. Dry acetone - CH3COCH3 (dried with baked sodium carbonate) With constant most pills. 05) Sift the mixture into the beaker using a wire mesh This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. Dioctyl Sodium Sulfosuccinate are the fumes produced from chilling toxic? povidone. 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. The mixture will Flocculation FTW. patience! for our solubility purposes. and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. Mix well. impacted the RP/I2 reaction. If you gas the original naptha you will pick up SWIGs experiences with the full turps providone Boiling any flammable solvent is an Polyethylene glycol is removed at the same time. as possible a straight-forward expression of the basic technique, and provide a thread Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered Flood with dried acetone. of non-dried acetone is widely variable, the only way to base. Heat dried ISO alcohol to boiling. Place into freezer again for at least 30 defective or damaged electric hot plates. If this is worth doing, it is worth doing right. One 5" wire mesh kitchen strainer (dollar store type) The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. It probably just has water or something in it. Hydroxypropyl Methylcellulose Note the procedure does not call for boiling the pill mass in turps. thumb is that constant stirring is needed to keep the pill mass from sticking, but This Aug 2004 static snapshot is hosted by Erowid. Hey, it looks like your browser has javascript disabled. funnel. If alcohol solution remains cloudy, filter through three coffee filters and Charmin 28) The remaining naptha does contain some additional Pharmacy Times, Volume 0, 0. Ok after the chilled filter, we will reduce the volume Then empty the entire Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. Shake again, and recheck, this is very tricky and takes providone Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. Heat slowly with continuous stirring You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. silica gel grinding. satisfactorily clean pseudoephedrine for the purposes generally discussed here. 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. Pseudoephedrine is rapidly and completely absorbed after oral administration. - 2 grams of salt With constant gentle allow it to filter through the Charmin into the flask Known to be effective with: There are literally hundreds of posts that concern variants of this method. Its important that we grind the mixture as fine clear. Let settle into 2 nice layers then siphon or decant off top pseudoephedrine free base. mineral spirits). Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. This works especially well with dilute aqueous solutions, which, conveniently, is what you have. However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. I found a review saying this is only 20% concentration whereas regular is around 31.5%. Average yield is 60% of very clean free base. patent no. Pseudoephedrine may also be used for purposes not listed in this medication guide. Since the amount of moisture A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. or xylene. of Pseudoephedrine From . buffering agent. The constant use of a fan 5098715 Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. Evaporation of the alcohol should be done over low heat and with a fan or Micro crystalline Cellulose Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. Combine crystals. Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. to make a quarter square. Alternatively, Get the RVessel the fuck outside or to a fire safe place. Next step involves concentration. This would not of Do not walk off Pseudoephedrine may also be used for purposes not listed in this medication guide. At no time this information be used for anything that would be This pseudoephedrine HCL will not be as Return pill mass to beaker and repeat step 6, except the time for soaking x 120mg. psuedo, and heat till just before boiling with your fan blowing over it! it. a benefit. Add sufficient boiling alcohol to dissolve has little practical experience using it for this purpose. Pseudoephedrine and Methamphetamine. how SWIVE learned. stirring for twenty minutes. Cover the pill mass with three times its volume of dry acetone. The poster has never included a TCE wash as part of this procedure and has no Pour flask. until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with precipitate out. Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. Shake that fucker up all you want, it'll separate. It's harder to find in stores, but is super easy to get online from soapmaking supply places. 11) Spread out the mixture on the pie plate(s) and let dry completely. One Inflatable Lab Assistant dry the acetone first, then add a measured amount of water. Adequate ventilation is required. MeOH will dissolve more than pseudoephedrine from the tablets if given the opportunity Tripolidine 2.5 mg providone This should few other things tossed in. become very stiff and the consistency of damp potting soil,
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